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The content of the Class I component began to decrease when heated to -50°C, and meanwhile the Class II component began to increase and leached a level of ~60% at 66°C
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Steady-state measurements Three-hundred scans per sample were taken, averaged, apodized with a Happ-Genzel function, and Fourier transformed to give a final resolution of 2 cm^sup -1^
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6 ms and δ = 450 µs is significantly above zero
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